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1 article(s) from Julien, Patrick A

The effect of milling frequency on a mechanochemical organic reaction monitored by in situ Raman spectroscopy

Patrick A. Julien,
Ivani Malvestiti and
Tomislav Friščić

Beilstein J. Org. Chem. 2017, 13, 2160–2168, doi:10.3762/bjoc.13.216

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Scheme 1: Milling synthesis of 2,3-diphenylquinoxaline from benzil and ortho-phenylenediamine [40].

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Scheme 2: Movement of the milling jar and sample holder under milling conditions.

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Figure 1: Time-resolved Raman spectrum for the double condensation of o-phenylenediamine and benzil to form 2...

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Figure 2: Section of the time-resolved Raman spectrum for the model mechanochemical reaction conducted at 30 ...

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Figure 3: (Left) Estimated contribution of each component for each Raman spectrum over time of the synthesis ...

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Figure 4: The effect of milling frequency on the milling condensation of benzil and o-phenylenediamine to for...

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Figure 5: The reproducibility of varying milling frequency on the neat mechanochemical condensation of benzil...

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Figure 6: The effect of milling frequency on the internal jar temperature measured immediately after reaction...

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Published 18 Oct 2017

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